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Precise determination of crystal lattice parameters


Federal Scientific Research Center "Crystallography and Photonics", Russian Academy of Sciences, Shubnikov Institute of Crystallography, Russian Academy of Sciences, Leninskii prosp. 59, Moscow, 119333, Russian Federaion

Precision X-ray methods for absolute and relative determination of crystal lattice parameters (interplanar distances) are described and compared, including the X-ray divergent-beam (Kossel) technique, the Bond method, the Renninger method, the back reflection method, the interference method, and the method of standards. It is shown that for most of the considered methods, a relative accuracy of ~10−5—10−6 for determining the lattice parameters is usually achievable, with the last two methods giving a much greater accuracy, at the level of ~10−8—10−9.

Fulltext is available at IOP
Keywords: X-ray radiation, diffraction, Bragg angle, crystal lattice parameter, interplane distance
PACS: 06.20.Jr, 07.85.−m, 61.05.cp, 61.50.−f (all)
DOI: 10.3367/UFNe.2019.07.038599
URL: https://ufn.ru/en/articles/2020/9/d/
Citation: Lider V V "Precise determination of crystal lattice parameters" Phys. Usp. 63 907–928 (2020)
BibTexBibNote ® (generic)BibNote ® (RIS)Medline RefWorks
RT Journal
T1 Precise determination of crystal lattice parameters
A1 Lider,V.V.
PB Physics-Uspekhi
PY 2020
FD 10 Sep, 2020
JF Physics-Uspekhi
JO Phys. Usp.
VO 63
IS 9
SP 907-928
DO 10.3367/UFNe.2019.07.038599
LK https://ufn.ru/en/articles/2020/9/d/

Received: 14th, May 2019, revised: 1st, July 2019, 2nd, July 2019

Оригинал: Лидер В В «Прецизионное определение параметров кристаллической решётки» УФН 190 971–994 (2020); DOI: 10.3367/UFNr.2019.07.038599

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